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Colin Judge: Testing structural materials in Idaho’s newest hot cell facility
Idaho National Laboratory’s newest facility—the Sample Preparation Laboratory (SPL)—sits across the road from the Hot Fuel Examination Facility (HFEF), which started operating in 1975. SPL will host the first new hot cells at INL’s Materials and Fuels Complex (MFC) in 50 years, giving INL researchers and partners new flexibility to test the structural properties of irradiated materials fresh from the Advanced Test Reactor (ATR) or from a partner’s facility.
Materials meant to withstand extreme conditions in fission or fusion power plants must be tested under similar conditions and pushed past their breaking points so performance and limitations can be understood and improved. Once irradiated, materials samples can be cut down to size in SPL and packaged for testing in other facilities at INL or other national laboratories, commercial labs, or universities. But they can also be subjected to extreme thermal or corrosive conditions and mechanical testing right in SPL, explains Colin Judge, who, as INL’s division director for nuclear materials performance, oversees SPL and other facilities at the MFC.
SPL won’t go “hot” until January 2026, but Judge spoke with NN staff writer Susan Gallier about its capabilities as his team was moving instruments into the new facility.
J. Ambrosek, M. Anderson, K. Sridharan, T. Allen
Nuclear Technology | Volume 165 | Number 2 | February 2009 | Pages 166-173
Technical Paper | Thermal Hydraulics | doi.org/10.13182/NT165-166
Articles are hosted by Taylor and Francis Online.
A compilation and reevaluation of data from the 1950s and 1970s from three forced convective heat transfer experiments using the ternary fluoride salt FLiNaK (46.5 LiF-11.5 NaF-42 KF mol%) using presently known thermophysical properties of this salt has been performed. The previous experiments each analyzed their data using different values for the properties of the liquid salt, thus leading to differences in the reported heat transfer coefficients. For turbulent flow in experiments conducted in chambers constructed of Inconel® alloys (as used in these three previous experiments), it was determined that FLiNaK salt behaves as a "normal" fluid and can be modeled using the Dittus-Boelter (DB) correlation within ±15% accuracy. The DB correlation can thus be used for preliminary calculations of salt heat transfer. Despite the success of the DB correlation for tests conducted in Inconel® chambers, forced convective data on heat transfer in nickel and Type 316 stainless steel produced different results. The physical effects contributing to the difference in the data measured in different container materials are not understood. The concentration of Cr (the main corrosion product added to the salt during a test) is similar between Inconel® alloys and Type 316 stainless steel and should affect each test similarly. Nickel is a relatively inert container material to fluoride salts and should not affect the heat transfer. To reconcile the experiments, a simplified approach was undertaken to determine if the radiant heat transfer to the FLiNaK salt could account for the differences. It was found that under the experimental conditions used by previous investigators, the radiant heat transfer from container to salt was <2%. However, the amount of energy transferred by radiation can be significant in applications involving high temperatures (T = 1123 K) and laminar flow conditions (Re < 500) in pipes with a diameter of 1 cm or greater.