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Colin Judge: Testing structural materials in Idaho’s newest hot cell facility
Idaho National Laboratory’s newest facility—the Sample Preparation Laboratory (SPL)—sits across the road from the Hot Fuel Examination Facility (HFEF), which started operating in 1975. SPL will host the first new hot cells at INL’s Materials and Fuels Complex (MFC) in 50 years, giving INL researchers and partners new flexibility to test the structural properties of irradiated materials fresh from the Advanced Test Reactor (ATR) or from a partner’s facility.
Materials meant to withstand extreme conditions in fission or fusion power plants must be tested under similar conditions and pushed past their breaking points so performance and limitations can be understood and improved. Once irradiated, materials samples can be cut down to size in SPL and packaged for testing in other facilities at INL or other national laboratories, commercial labs, or universities. But they can also be subjected to extreme thermal or corrosive conditions and mechanical testing right in SPL, explains Colin Judge, who, as INL’s division director for nuclear materials performance, oversees SPL and other facilities at the MFC.
SPL won’t go “hot” until January 2026, but Judge spoke with NN staff writer Susan Gallier about its capabilities as his team was moving instruments into the new facility.
Stephen Priebe, Ken Bateman
Nuclear Technology | Volume 162 | Number 2 | May 2008 | Pages 199-207
Technical Paper | First International Pyroprocessing Research Conference | doi.org/10.13182/NT08-A3948
Articles are hosted by Taylor and Francis Online.
The treatment of spent nuclear fuel for disposition using an electrometallurgical technique results in two high-level waste forms: a ceramic waste form (CWF) and a metal waste form. Reactive metal fuel constituents, including all of the transuranic metals and the majority of the fission products, remain in the salt as chlorides and are processed into the CWF. The solidified salt is containerized and transferred to the CWF process, where it is ground in an argon atmosphere. Zeolite 4A is dried in a mechanically fluidized dryer to ~0.1 wt% moisture and ground to a particle-size range of 45 to 250 m. The salt and zeolite are mixed in a V-mixer and heated to 500°C for ~18 h to occlude the salt into the structure of the zeolite. The salt-loaded zeolite is cooled, mixed with borosilicate glass frit, and transferred to a crucible, which is placed in a furnace and heated to 925°C. During this process, known as pressureless consolidation, the zeolite is converted to the final sodalite form and the glass thoroughly encapsulates the sodalite, producing a dense, leach-resistant final waste form. During the last several years, changes have occurred to the process, including particle size of input materials and conversion from hot isostatic pressing to pressureless consolidation. This paper is intended to provide the current status of the CWF process, focusing on the adaptation to pressureless consolidation. Discussions include impacts of particle size on final waste form and the pressureless consolidation cycle. A model is presented that shows the heating and cooling cycles and the effect of radioactive decay heat on the amount of fission products that can be incorporated into the CWF.