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Colin Judge: Testing structural materials in Idaho’s newest hot cell facility
Idaho National Laboratory’s newest facility—the Sample Preparation Laboratory (SPL)—sits across the road from the Hot Fuel Examination Facility (HFEF), which started operating in 1975. SPL will host the first new hot cells at INL’s Materials and Fuels Complex (MFC) in 50 years, giving INL researchers and partners new flexibility to test the structural properties of irradiated materials fresh from the Advanced Test Reactor (ATR) or from a partner’s facility.
Materials meant to withstand extreme conditions in fission or fusion power plants must be tested under similar conditions and pushed past their breaking points so performance and limitations can be understood and improved. Once irradiated, materials samples can be cut down to size in SPL and packaged for testing in other facilities at INL or other national laboratories, commercial labs, or universities. But they can also be subjected to extreme thermal or corrosive conditions and mechanical testing right in SPL, explains Colin Judge, who, as INL’s division director for nuclear materials performance, oversees SPL and other facilities at the MFC.
SPL won’t go “hot” until January 2026, but Judge spoke with NN staff writer Susan Gallier about its capabilities as his team was moving instruments into the new facility.
Hiroshi Sugai, Kenzo Munakata
Nuclear Technology | Volume 99 | Number 2 | August 1992 | Pages 235-241
Technical Paper | Enrichment and Reprocessing System | doi.org/10.13182/NT92-A34693
Articles are hosted by Taylor and Francis Online.
In solvent extraction for nuclear fuel reprocessing, a stable emulsion called “crud” is formed at the interface between the organic and aqueous phases. Crud is an emulsion stabilized by finely dispersed solids. Process disturbances are often induced by crud. Accordingly, crud should be eliminated from the interface in the extractors. The eliminated crud is stable and highly radioactive; thus, the treatment of this crud may be difficult. Complexes of zirconium and tributyl phosphate (TBP) degradation products, such as phosphoric acid (H3PO4) and mono-n-butyl phosphate (H2MBP), are one source of the fine particles that stabilize emulsions in the extraction process. A chemical treatment method to demulsify crud stabilized by precipitates of Zr-H3PO4 and Zr-H2MBP is studied. Experimental results indicate that neutralization by an alkaline solution, particularly sodium carbonate, is very effective for the destruction of this crud.
