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Nuclear Energy Conference & Expo (NECX)
September 8–11, 2025
Atlanta, GA|Atlanta Marriott Marquis
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Inkjet droplets of radioactive material enable quick, precise testing at NIST
Researchers at the National Institute of Standards and Technology have developed a technique called cryogenic decay energy spectrometry capable of detecting single radioactive decay events from tiny material samples and simultaneously identifying the atoms involved. In time, the technology could replace characterization tasks that have taken months and could support rapid, accurate radiopharmaceutical development and used nuclear fuel recycling, according to an article published on July 8 by NIST.
Tsutomu Sakurai, Akira Takahashi, Niro Ishikawa, Yoshihide Komaki
Nuclear Technology | Volume 83 | Number 1 | October 1988 | Pages 24-30
Technical Paper | Fuel Cycle | doi.org/10.13182/NT88-A34172
Articles are hosted by Taylor and Francis Online.
The composition of NOx generated in the dissolution of UO2 has been described in different ways by earlier authors. Finding a way to determine the NOx composition in the dissolution included experiments concerning the reactions of NO and NO2 with 3 to 6 M HNO3. The following conclusions have been obtained for the dissolution: (a) of the NOx, NO is the direct product of the dissolution [3UO2 + 8HNO3 → 3UO2(NO3)2 + 2NO + 4H2O]; (b) part of the NO is converted quickly to NO2 by the second reaction, i.e., NO + 2HNO3→ 3NO2 + H2O (the equilibrium constant of this reaction determines the NOx composition); (c) the dissolution is therefore expressible as 3UO2 + 4(2 + x)HNO3→3UO2(NO3)2 + 2(1 — x)NO + 6xNO2 + 2(2 + x)H2O, (0 < × < 1) (some values of the × were obtained); (d) the amount of NO2 in the NOx is considerably smaller than that reported by earlier authors, e.g., 25% for 6.7 MHNO3 at 101°C; (e) UO2(NO3)2 coexisting in the solution tends to increase the NO component in the NOx.
