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Colin Judge: Testing structural materials in Idaho’s newest hot cell facility
Idaho National Laboratory’s newest facility—the Sample Preparation Laboratory (SPL)—sits across the road from the Hot Fuel Examination Facility (HFEF), which started operating in 1975. SPL will host the first new hot cells at INL’s Materials and Fuels Complex (MFC) in 50 years, giving INL researchers and partners new flexibility to test the structural properties of irradiated materials fresh from the Advanced Test Reactor (ATR) or from a partner’s facility.
Materials meant to withstand extreme conditions in fission or fusion power plants must be tested under similar conditions and pushed past their breaking points so performance and limitations can be understood and improved. Once irradiated, materials samples can be cut down to size in SPL and packaged for testing in other facilities at INL or other national laboratories, commercial labs, or universities. But they can also be subjected to extreme thermal or corrosive conditions and mechanical testing right in SPL, explains Colin Judge, who, as INL’s division director for nuclear materials performance, oversees SPL and other facilities at the MFC.
SPL won’t go “hot” until January 2026, but Judge spoke with NN staff writer Susan Gallier about its capabilities as his team was moving instruments into the new facility.
Tsutomu Sakurai, Akira Takahashi, Niro Ishikawa, Yoshihide Komaki
Nuclear Technology | Volume 83 | Number 1 | October 1988 | Pages 24-30
Technical Paper | Fuel Cycle | doi.org/10.13182/NT88-A34172
Articles are hosted by Taylor and Francis Online.
The composition of NOx generated in the dissolution of UO2 has been described in different ways by earlier authors. Finding a way to determine the NOx composition in the dissolution included experiments concerning the reactions of NO and NO2 with 3 to 6 M HNO3. The following conclusions have been obtained for the dissolution: (a) of the NOx, NO is the direct product of the dissolution [3UO2 + 8HNO3 → 3UO2(NO3)2 + 2NO + 4H2O]; (b) part of the NO is converted quickly to NO2 by the second reaction, i.e., NO + 2HNO3→ 3NO2 + H2O (the equilibrium constant of this reaction determines the NOx composition); (c) the dissolution is therefore expressible as 3UO2 + 4(2 + x)HNO3→3UO2(NO3)2 + 2(1 — x)NO + 6xNO2 + 2(2 + x)H2O, (0 < × < 1) (some values of the × were obtained); (d) the amount of NO2 in the NOx is considerably smaller than that reported by earlier authors, e.g., 25% for 6.7 MHNO3 at 101°C; (e) UO2(NO3)2 coexisting in the solution tends to increase the NO component in the NOx.