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Colin Judge: Testing structural materials in Idaho’s newest hot cell facility
Idaho National Laboratory’s newest facility—the Sample Preparation Laboratory (SPL)—sits across the road from the Hot Fuel Examination Facility (HFEF), which started operating in 1975. SPL will host the first new hot cells at INL’s Materials and Fuels Complex (MFC) in 50 years, giving INL researchers and partners new flexibility to test the structural properties of irradiated materials fresh from the Advanced Test Reactor (ATR) or from a partner’s facility.
Materials meant to withstand extreme conditions in fission or fusion power plants must be tested under similar conditions and pushed past their breaking points so performance and limitations can be understood and improved. Once irradiated, materials samples can be cut down to size in SPL and packaged for testing in other facilities at INL or other national laboratories, commercial labs, or universities. But they can also be subjected to extreme thermal or corrosive conditions and mechanical testing right in SPL, explains Colin Judge, who, as INL’s division director for nuclear materials performance, oversees SPL and other facilities at the MFC.
SPL won’t go “hot” until January 2026, but Judge spoke with NN staff writer Susan Gallier about its capabilities as his team was moving instruments into the new facility.
Yuezhou Wei, Mikio Kumagai, Yoichi Takashima, Giuseppe Modolo, Reinhard Odoj
Nuclear Technology | Volume 132 | Number 3 | December 2000 | Pages 413-423
Technical Paper | Reprocessing | doi.org/10.13182/NT00-A3154
Articles are hosted by Taylor and Francis Online.
To develop an advanced partitioning process by extraction chromatography using a minimal organic solvent and compact equipment to separate minor actinides such as Am and Cm from nitrate acidic high-level waste (HLW) solution, several novel silica-based extraction resins have been prepared by impregnating organic extractants into the styrene-divinylbenzene copolymer, which is immobilized in porous silica particles (SiO2-P). The extractants include octyl(phenyl)-N, N-diisobutylcarbamoylmethylphosphine oxide (CMPO), di(2-ethylhexyl)-phosphoric acid (HDEHP), and bis(2,4,4-trimethylpentyl)dithiophosphinic acid (Cyanex 301). Compared to conventional polymer-matrix resins, these new types of extraction resin are characterized by rapid kinetics and significantly low pressure loss in a packed column.The results of separation experiments revealed that trivalent actinides and lanthanides can be separated from other fission products, such as Cs, Sr, and Ru in simulated HLW solution containing concentrated nitric acid by extraction chromatography using a CMPO/SiO2-P resin-packed column. Satisfactory separation between Am(III) and a macro amount of lanthanides from simulated HLW solution with pH 4 was achieved by using a newly purified Cyanex 301/SiO2-P resin. However, the Am(III) separation was very sensitive to the purity of Cyanex 301, and the improvement of its stability is an important task for practical utilization.