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Colin Judge: Testing structural materials in Idaho’s newest hot cell facility
Idaho National Laboratory’s newest facility—the Sample Preparation Laboratory (SPL)—sits across the road from the Hot Fuel Examination Facility (HFEF), which started operating in 1975. SPL will host the first new hot cells at INL’s Materials and Fuels Complex (MFC) in 50 years, giving INL researchers and partners new flexibility to test the structural properties of irradiated materials fresh from the Advanced Test Reactor (ATR) or from a partner’s facility.
Materials meant to withstand extreme conditions in fission or fusion power plants must be tested under similar conditions and pushed past their breaking points so performance and limitations can be understood and improved. Once irradiated, materials samples can be cut down to size in SPL and packaged for testing in other facilities at INL or other national laboratories, commercial labs, or universities. But they can also be subjected to extreme thermal or corrosive conditions and mechanical testing right in SPL, explains Colin Judge, who, as INL’s division director for nuclear materials performance, oversees SPL and other facilities at the MFC.
SPL won’t go “hot” until January 2026, but Judge spoke with NN staff writer Susan Gallier about its capabilities as his team was moving instruments into the new facility.
Haruo Sato
Nuclear Technology | Volume 127 | Number 2 | August 1999 | Pages 199-211
Technical Paper | Radioactive Waste Management and Disposal | doi.org/10.13182/NT127-199
Articles are hosted by Taylor and Francis Online.
The diffusion of radionuclides into the pore spaces of a rock matrix and the pore properties in fractured crystalline rocks were studied. The work concentrated on the predominant water-conducting fracture system in the host granodiorite of the Kamaishi In Situ Test Site, which consists of fracture fillings and altered granodiorite. Through-diffusion experiments to obtain effective and apparent diffusion coefficients (De and Da, respectively) for Na+, Cs+, HTO, Cl-, and SeO32- as a function of ionic charge were conducted through the fracture fillings and altered and intact granodiorite. The total porosity , density, pore-size distribution, and specific surface area of the pores of the rocks were also determined by a water saturation method and Hg porosimetry. The average is, in the order from highest to lowest, as follows: fracture fillings (5.6%) greater than altered granodiorite (3.2%) greater than intact granodiorite (2.3%), and gradually it decreases into the matrix. The pore sizes of the intact and altered granodiorite range from 10 nm to 200 m, and the fracture fillings from 50 nm to 200 m, but almost all pores are found around 0.1 and 200 m in the fracture fillings. The De values for all species are in the following order: fracture fillings greater than altered granodiorite greater than intact granodiorite, as with the rock porosity. In addition, no effect of ionic charge on De is found. No significant dependence for Da values on the rock porosity is found. The formation factors FF and geometric factors G of the rocks were evaluated by normalizing the free water diffusion coefficient Do for each species. The FF decreased with decreasing rock porosity, and an empirical equation for the rock porosity was derived to be FF = 1.57±0.02. The G values showed a tendency to slightly decrease with decreasing rock porosity, but they were approximately constant (0.12 to 0.19) in this porosity range. This indicates that accessible pores decrease into the rock matrix from the fractures, and diffusion is also reduced into the rock matrix. Furthermore, it was concluded that a simplified model based on FF and Do values is approximately reasonable to predict De.