Ten critical assemblies of enriched uranyl-fluoride heavy-water solutions have been studied. In six cases, heavy water reflectors surrounded solutions in which the atomic ratio of deuterium to uranium-235 varied from 34 to 430. The remaining four assemblies were without reflector and the deuterium to U235 ratio ranged from 230 to 2080. Activation rates within the systems were measured for the resonance detectors In, Au, Pd, and Mn and for the fission detectors U235, U238, Pu239, and U233.