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Colin Judge: Testing structural materials in Idaho’s newest hot cell facility
Idaho National Laboratory’s newest facility—the Sample Preparation Laboratory (SPL)—sits across the road from the Hot Fuel Examination Facility (HFEF), which started operating in 1975. SPL will host the first new hot cells at INL’s Materials and Fuels Complex (MFC) in 50 years, giving INL researchers and partners new flexibility to test the structural properties of irradiated materials fresh from the Advanced Test Reactor (ATR) or from a partner’s facility.
Materials meant to withstand extreme conditions in fission or fusion power plants must be tested under similar conditions and pushed past their breaking points so performance and limitations can be understood and improved. Once irradiated, materials samples can be cut down to size in SPL and packaged for testing in other facilities at INL or other national laboratories, commercial labs, or universities. But they can also be subjected to extreme thermal or corrosive conditions and mechanical testing right in SPL, explains Colin Judge, who, as INL’s division director for nuclear materials performance, oversees SPL and other facilities at the MFC.
SPL won’t go “hot” until January 2026, but Judge spoke with NN staff writer Susan Gallier about its capabilities as his team was moving instruments into the new facility.
Muhammad Abdullah, Ahmad Ali, Riaz Khan, Osama Abdur Rehman, Zia-ur- Rehman, Shahab Ud-Din Khan, Sehrish Shakir, Shahzaib Zahid, Muhammad Ismail, Rafaqat Ali, Sarfraz Ahmad, Shahid Hussain
Fusion Science and Technology | Volume 80 | Number 6 | August 2024 | Pages 731-740
Research Article | doi.org/10.1080/15361055.2023.2241004
Articles are hosted by Taylor and Francis Online.
The MT-II is a small spherical tokamak that is currently under construction at the Pakistan Tokamak Plasma Research Institute. Wall conditioning of the MT-II vacuum vessel (VV) is an essential step to achieve a good quality vacuum for plasma experiments. This study presents an overview of the wall-conditioning techniques implemented on the MT-II VV, including baking and glow discharge cleaning (GDC). Prior to wall conditioning, the system is checked via a helium leak test machine and residual gas analyzer (RGA) to identify and remove leaks. The VV walls are baked at ~180 °C to get rapid desorption of water vapors and other impurities. After the baking process, the partial pressure of most of the carbon- and oxygen-containing impurities is reduced. In particular, the partial pressure of water vapors is reduced by 93%. Consequently, the total leak and outgassing rate is significantly reduced. To further improve the vacuum condition in the vessel, hydrogen GDC is carried out. The fill hydrogen pressure and anode voltage are optimized to get a stable glow discharge. The RGA scan shows that GDC reduces the partial pressure of H2O, O2, and CO2 by 57%, 63%, and 51%, respectively. The results signify that baking and GDC are effective techniques for wall conditioning of the MT-II VV.