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Colin Judge: Testing structural materials in Idaho’s newest hot cell facility
Idaho National Laboratory’s newest facility—the Sample Preparation Laboratory (SPL)—sits across the road from the Hot Fuel Examination Facility (HFEF), which started operating in 1975. SPL will host the first new hot cells at INL’s Materials and Fuels Complex (MFC) in 50 years, giving INL researchers and partners new flexibility to test the structural properties of irradiated materials fresh from the Advanced Test Reactor (ATR) or from a partner’s facility.
Materials meant to withstand extreme conditions in fission or fusion power plants must be tested under similar conditions and pushed past their breaking points so performance and limitations can be understood and improved. Once irradiated, materials samples can be cut down to size in SPL and packaged for testing in other facilities at INL or other national laboratories, commercial labs, or universities. But they can also be subjected to extreme thermal or corrosive conditions and mechanical testing right in SPL, explains Colin Judge, who, as INL’s division director for nuclear materials performance, oversees SPL and other facilities at the MFC.
SPL won’t go “hot” until January 2026, but Judge spoke with NN staff writer Susan Gallier about its capabilities as his team was moving instruments into the new facility.
K. Holtrop, D. Buchenauer, C. Chrobak, C. Murphy, R. Nygren, E. Unterberg, M. Zach
Fusion Science and Technology | Volume 72 | Number 4 | November 2017 | Pages 634-639
Technical Paper | doi.org/10.1080/15361055.2017.1347456
Articles are hosted by Taylor and Francis Online.
Future tokamak devices are envisioned to utilize a high-Z metal divertor with tungsten as the leading candidate. However, tokamak experiments with tungsten divertors have seen significant detrimental effects on plasma performance. The DIII-D tokamak presently has carbon as the plasma facing surface but to study the effect of tungsten on the plasma and its migration around the vessel, two toroidal rows of carbon tiles in the divertor region were modified with high-Z metal inserts, composed of a molybdenum alloy (TZM) coated with tungsten. A dedicated two week experimental campaign was run with the high-Z metal inserts. One row was coated with tungsten containing naturally occurring levels of isotopes. The second row was coated with tungsten where the isotope 182W was enhanced from the natural level of 26% up to greater than 90%. The different isotopic concentrations enabled the experiment to differentiate between the two different sources of metal migration from the divertor. Various coating methods were explored for the deposition of the tungsten coating, including chemical vapor deposition, electroplating, vacuum plasma spray, and electron beam physical vapor deposition. The coatings were tested to see if they were robust enough to act as a divertor target for the experiment. Tests included cyclic thermal heating using a high power laser and high-fluence deuterium plasma bombardment. The issues associate with the design of the inserts (tile installation, thermal stress, arcing, leading edges, surface preparation, etc.), are reviewed. The results of the tests used to select the coating method and preliminary experimental observations are presented.