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Colin Judge: Testing structural materials in Idaho’s newest hot cell facility
Idaho National Laboratory’s newest facility—the Sample Preparation Laboratory (SPL)—sits across the road from the Hot Fuel Examination Facility (HFEF), which started operating in 1975. SPL will host the first new hot cells at INL’s Materials and Fuels Complex (MFC) in 50 years, giving INL researchers and partners new flexibility to test the structural properties of irradiated materials fresh from the Advanced Test Reactor (ATR) or from a partner’s facility.
Materials meant to withstand extreme conditions in fission or fusion power plants must be tested under similar conditions and pushed past their breaking points so performance and limitations can be understood and improved. Once irradiated, materials samples can be cut down to size in SPL and packaged for testing in other facilities at INL or other national laboratories, commercial labs, or universities. But they can also be subjected to extreme thermal or corrosive conditions and mechanical testing right in SPL, explains Colin Judge, who, as INL’s division director for nuclear materials performance, oversees SPL and other facilities at the MFC.
SPL won’t go “hot” until January 2026, but Judge spoke with NN staff writer Susan Gallier about its capabilities as his team was moving instruments into the new facility.
S. Le Tacon, A. Brodier, C. Chicanne, M. Theobald
Fusion Science and Technology | Volume 70 | Number 2 | August-September 2016 | Pages 351-357
Technical Paper | doi.org/10.13182/FST15-240
Articles are hosted by Taylor and Francis Online.
Some experiments implemented on the Laser Megajoule facility (LMJ) require the use of the rare-earth (RE) elements, the lanthanides (57 < Z < 71). Rare-earth metals are known to be unstable under atmospheric conditions and some of them are extremely reactive with air. They may react with oxygen and humidity to form RE oxides. In the present work, we study the oxidation of different RE thin films (gadolinium, dysprosium, and praseodymium) prepared by physical vapor deposition. Energy-dispersion spectroscopy, scanning electron microscopy, Rutherford backscattering spectroscopy, and weight measurement are performed to characterize the corrosion mechanisms as a function of time and aging atmospheres (air, dry box, and vacuum). It appears that the oxidation kinetics depends on atomic number and microstructure of the films. Praseodymium coatings are very quickly corroded (in a few hours) when exposed to air and degrade to a yellow powder. Aluminum layers, used as a diffusion barrier, allow us to preserve praseodymium coatings over a period of several weeks when aging in a dry box. Gadolinium and dysprosium coatings (without a protective layer) are preserved from corrosion due to the formation of a passivation layer on their surface. Whatever Z, a dense microstructure permits us to limit the oxygen content and allows us to stabilize the residual stress.