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Colin Judge: Testing structural materials in Idaho’s newest hot cell facility
Idaho National Laboratory’s newest facility—the Sample Preparation Laboratory (SPL)—sits across the road from the Hot Fuel Examination Facility (HFEF), which started operating in 1975. SPL will host the first new hot cells at INL’s Materials and Fuels Complex (MFC) in 50 years, giving INL researchers and partners new flexibility to test the structural properties of irradiated materials fresh from the Advanced Test Reactor (ATR) or from a partner’s facility.
Materials meant to withstand extreme conditions in fission or fusion power plants must be tested under similar conditions and pushed past their breaking points so performance and limitations can be understood and improved. Once irradiated, materials samples can be cut down to size in SPL and packaged for testing in other facilities at INL or other national laboratories, commercial labs, or universities. But they can also be subjected to extreme thermal or corrosive conditions and mechanical testing right in SPL, explains Colin Judge, who, as INL’s division director for nuclear materials performance, oversees SPL and other facilities at the MFC.
SPL won’t go “hot” until January 2026, but Judge spoke with NN staff writer Susan Gallier about its capabilities as his team was moving instruments into the new facility.
Yasunori Iwai, Katsumi Sato, Toshihiko Yamanishi
Fusion Science and Technology | Volume 66 | Number 1 | July-August 2014 | Pages 214-220
Technical Paper | doi.org/10.13182/FST13-725
Articles are hosted by Taylor and Francis Online.
We have developed a honeycomb palladium catalyst to be used for the oxidation of tritiated hydrocarbons. Since the suitable loading rate of palladium deposited on the base material is a technical point, honeycomb-shaped palladium catalysts of three different loading rates—2, 5, and 10 g/L—were prepared to investigate the effect of loading rate of palladium on reaction rate in this study. Tritiated methane was selected as the typical hydrocarbon. A 12 m3 tank was prepared to prevent tritiated methane at tracer concentration fed to the catalytic reactor from fluctuating. The overall reaction rate constant for tritiated methane oxidation on the honeycomb palladium catalyst was determined with a flow-through system as a function of space velocity from 1000 to 6300 h−1, methane concentration in carrier from 0.004 to 100 ppm, and temperature of catalyst from 322 to 673 K. The honeycomb palladium catalyst without pretreatment for activation initially lowers the overall reaction rate constant at lower temperatures. However, the constant recovers steeply to the original value during the continuous combustion of tritiated methane. The loading rate of palladium deposited on the base material has little effect on reaction rate for tritiated methane combustion. The overall reaction rate constant is proportional to the space velocity. The overall reaction rate constant is independent on the methane concentration when it is less than 10 ppm.
