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Colin Judge: Testing structural materials in Idaho’s newest hot cell facility
Idaho National Laboratory’s newest facility—the Sample Preparation Laboratory (SPL)—sits across the road from the Hot Fuel Examination Facility (HFEF), which started operating in 1975. SPL will host the first new hot cells at INL’s Materials and Fuels Complex (MFC) in 50 years, giving INL researchers and partners new flexibility to test the structural properties of irradiated materials fresh from the Advanced Test Reactor (ATR) or from a partner’s facility.
Materials meant to withstand extreme conditions in fission or fusion power plants must be tested under similar conditions and pushed past their breaking points so performance and limitations can be understood and improved. Once irradiated, materials samples can be cut down to size in SPL and packaged for testing in other facilities at INL or other national laboratories, commercial labs, or universities. But they can also be subjected to extreme thermal or corrosive conditions and mechanical testing right in SPL, explains Colin Judge, who, as INL’s division director for nuclear materials performance, oversees SPL and other facilities at the MFC.
SPL won’t go “hot” until January 2026, but Judge spoke with NN staff writer Susan Gallier about its capabilities as his team was moving instruments into the new facility.
Y. Belot, H. Camus, T. Marini
Fusion Science and Technology | Volume 21 | Number 2 | March 1992 | Pages 556-559
Safety; Measurement and Accountability; Operation and Maintenance; Application | doi.org/10.13182/FST92-A29805
Articles are hosted by Taylor and Francis Online.
Recent observations suggested that formaldehyde can be incorporated in vegetation at a very high rate. This encouraged our laboratory to develop a methodology for determining tritiated formaldehyde (CHTO) in gaseous effluents containing HTO and HT as dominant species. CHTO being very soluble in water is collected in a solution of carrier formaldehyde. This carrier is necessary for precipitating the formaldehyde derivative of dimedone and collecting it by filtration. The precipitate, which contains the formaldehyde hydrogens, is freed from exchangeable tritium, dried in a oven, and combusted to water for tritium determination. CHTO can thus be separated from HTO with a high efficiency, leading to the possibility of determining accurately 1 Bq of CHTO in as much as 5 × 104 Bq of HTO. The methodology has been applied in preliminary experiments to determine the ratio of CHTO to HTO in effluents from a tritium-handling facility and effluents released from solid miscellaneous wastes. The median of the ratio of CHTO to HTO was 1.2 × 10−3 for the tritium-handling facility (40 samples), and 4.5 × 10−4 for miscellaneous solid wastes (12 samples).