A polycrystalline palladium rod is electrolytically charged with deuterium up to a deuterium/palladium ratio of 0.81 while several sample parameters are simultaneously measured in situ, including electrical resistivity, sample dimensions, cell temperature, and neutron production. Various charging rates are used in an attempt to provoke any anomalous behavior, such as a previously unknown crystallographic or chemical phase change, that might account for reports of heat or neutron production. Neither the electrical resistivity nor sample dimensions manifest evidence of any anomaly.