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Colin Judge: Testing structural materials in Idaho’s newest hot cell facility
Idaho National Laboratory’s newest facility—the Sample Preparation Laboratory (SPL)—sits across the road from the Hot Fuel Examination Facility (HFEF), which started operating in 1975. SPL will host the first new hot cells at INL’s Materials and Fuels Complex (MFC) in 50 years, giving INL researchers and partners new flexibility to test the structural properties of irradiated materials fresh from the Advanced Test Reactor (ATR) or from a partner’s facility.
Materials meant to withstand extreme conditions in fission or fusion power plants must be tested under similar conditions and pushed past their breaking points so performance and limitations can be understood and improved. Once irradiated, materials samples can be cut down to size in SPL and packaged for testing in other facilities at INL or other national laboratories, commercial labs, or universities. But they can also be subjected to extreme thermal or corrosive conditions and mechanical testing right in SPL, explains Colin Judge, who, as INL’s division director for nuclear materials performance, oversees SPL and other facilities at the MFC.
SPL won’t go “hot” until January 2026, but Judge spoke with NN staff writer Susan Gallier about its capabilities as his team was moving instruments into the new facility.
C. A. Gentile, H. M. Fan, J. W. Hartfield, R. J. Hawryluk, F. Hegeler, P. J. Heitzenroeder, C. H. Jun, L. P. Ku, P. H. LaMarche, M. C. Myers, J. J. Parker, R. F. Parsells, M. Payen, S. Raftopoulos, J. D. Sethian
Fusion Science and Technology | Volume 43 | Number 3 | May 2003 | Pages 414-419
Technical Paper | Lasers and Heavy-Ion Drivers | doi.org/10.13182/FST03-A286
Articles are hosted by Taylor and Francis Online.
Princeton Plasma Physics Laboratory, in collaboration with the Naval Research Laboratory, is currently investigating various novel materials (single-crystal silicon, <100>, <110>, and <111>) for use as electron beam transmission windows in a krypton fluoride (KrF) excimer laser system. The primary function of the window is to isolate the active medium (excimer gas) from the excitation mechanism (field-emission diodes). The chosen window geometry must accommodate electron energy transfer >80% (750 keV) while maintaining the structural integrity during the mechanical load (1.3- to 2.0-atm base pressure differential, ~0.5-atm cyclic pressure amplitude, 5-Hz repetition rate) and the thermal load across the entire hibachi area (~0.9 Wcm-2). In addition, the window must be chemically resistant to attack by fluorine free radicals (hydrofluoric acid, secondary). In accordance with these structural, functional, and operational parameters, a 22.4-mm square silicon prototype window, coated with 500-nm thin-film silicon nitride (Si3N4), has been fabricated. The window consists of 81 square panes 0.019 ± 0.001 mm thick. The stiffened (orthogonal) sections are 0.065 mm wide and 0.500 mm thick (approximate). Assessment of silicon (and silicon nitride) material properties and computer-aided design modeling/analysis of the window design suggest that silicon may be a viable solution to inherent parameters and constraints.