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Colin Judge: Testing structural materials in Idaho’s newest hot cell facility
Idaho National Laboratory’s newest facility—the Sample Preparation Laboratory (SPL)—sits across the road from the Hot Fuel Examination Facility (HFEF), which started operating in 1975. SPL will host the first new hot cells at INL’s Materials and Fuels Complex (MFC) in 50 years, giving INL researchers and partners new flexibility to test the structural properties of irradiated materials fresh from the Advanced Test Reactor (ATR) or from a partner’s facility.
Materials meant to withstand extreme conditions in fission or fusion power plants must be tested under similar conditions and pushed past their breaking points so performance and limitations can be understood and improved. Once irradiated, materials samples can be cut down to size in SPL and packaged for testing in other facilities at INL or other national laboratories, commercial labs, or universities. But they can also be subjected to extreme thermal or corrosive conditions and mechanical testing right in SPL, explains Colin Judge, who, as INL’s division director for nuclear materials performance, oversees SPL and other facilities at the MFC.
SPL won’t go “hot” until January 2026, but Judge spoke with NN staff writer Susan Gallier about its capabilities as his team was moving instruments into the new facility.
A. Attalla, J. C. Birkbeck
Fusion Science and Technology | Volume 8 | Number 2 | September 1985 | Pages 2467-2470
Material Property and Tritium Control | Proceedings of the Second National Topical Meeting on Tritium Technology in Fission, Fusion and Isotopic Applications (Dayton, Ohio, April 30 to May 2, 1985) | doi.org/10.13182/FST85-A24649
Articles are hosted by Taylor and Francis Online.
A pulsed nuclear magnetic resonance (NMR) procedure was developed for the quantitative determination of deuterium and tritium in radioactive, effluent, wastewater to aid in the design of an efficient combined electrolytic/catalytic exchange system for the recovery of these hydrogen isotopes. The deuterium and tritium NMR signals were observed at 9.210 and 45.7 MHz, respectively. Ten different effluent water samples were analyzed for deuterium and tritium to establish base-line data for the preparation of standard reference samples. The hydrogen isotope concentrations ranged from 0.11 to 2.40 g deuterium and from 2.0 to 21.0 mg tritium per liter of processed sample. The standard deviation of the hydrogen isotope determinations is ±0.017 g deuterium and ±0.06 mg tritium per liter of processed effluent water. In the future, the effectiveness of specially prepared and analyzed (calorimetry) effluent samples as tritium standards will be investigated. *Mound is operated by Monsanto Research Corporation for the U. S. Department of Energy under Contract No. DE-AC04-76DP00053.
