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ANS Student Conference 2025
April 3–5, 2025
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Colin Judge: Testing structural materials in Idaho’s newest hot cell facility
Idaho National Laboratory’s newest facility—the Sample Preparation Laboratory (SPL)—sits across the road from the Hot Fuel Examination Facility (HFEF), which started operating in 1975. SPL will host the first new hot cells at INL’s Materials and Fuels Complex (MFC) in 50 years, giving INL researchers and partners new flexibility to test the structural properties of irradiated materials fresh from the Advanced Test Reactor (ATR) or from a partner’s facility.
Materials meant to withstand extreme conditions in fission or fusion power plants must be tested under similar conditions and pushed past their breaking points so performance and limitations can be understood and improved. Once irradiated, materials samples can be cut down to size in SPL and packaged for testing in other facilities at INL or other national laboratories, commercial labs, or universities. But they can also be subjected to extreme thermal or corrosive conditions and mechanical testing right in SPL, explains Colin Judge, who, as INL’s division director for nuclear materials performance, oversees SPL and other facilities at the MFC.
SPL won’t go “hot” until January 2026, but Judge spoke with NN staff writer Susan Gallier about its capabilities as his team was moving instruments into the new facility.
M. Glugla, T.L. Le, S. Gross, D. Niyongabo, R. Lsser, K.H. Simon
Fusion Science and Technology | Volume 41 | Number 3 | May 2002 | Pages 969-973
Purification and Chemical Process | Proceedings of the Sixth International Conference on Tritium Science and Technology Tsukuba, Japan November 12-16, 2001 | doi.org/10.13182/FST02-A22729
Articles are hosted by Taylor and Francis Online.
The principal techniques developed by different research groups for the detritiation of primary gaseous wastes are altogether based on processes with multiple stages comprising at least one step involving heterogeneously catalyzed chemical reactions. While the permeation of hydrogen isotopes through palladium/silver membranes combined with heterogeneously catalyzed reactions were proven to be particularly suitable for highly contaminated gases, isotopic swamping in a counter current mode is the method of choice in ITER for the final detritiation and recovery of residual amounts of tritium. Since the catalyst employed to promote the isotope exchange reactions should not support methanation of carbon monoxide and carbon dioxide an attempt was made to design a highly selective exchange catalyst. Amongst the catalysts screened with methane - deuterium exchange and carbon oxide - methanation as test reactions a high temperature reduced palladium/silica (SiO2) catalyst was found to match the selectivity requirements. However, even though the palladium/silica catalyst shows very little activity for methanation, carbon monoxide was found to obstruct the isotope exchange reaction, whereas carbon dioxide does not show this unwanted effect.
