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Colin Judge: Testing structural materials in Idaho’s newest hot cell facility
Idaho National Laboratory’s newest facility—the Sample Preparation Laboratory (SPL)—sits across the road from the Hot Fuel Examination Facility (HFEF), which started operating in 1975. SPL will host the first new hot cells at INL’s Materials and Fuels Complex (MFC) in 50 years, giving INL researchers and partners new flexibility to test the structural properties of irradiated materials fresh from the Advanced Test Reactor (ATR) or from a partner’s facility.
Materials meant to withstand extreme conditions in fission or fusion power plants must be tested under similar conditions and pushed past their breaking points so performance and limitations can be understood and improved. Once irradiated, materials samples can be cut down to size in SPL and packaged for testing in other facilities at INL or other national laboratories, commercial labs, or universities. But they can also be subjected to extreme thermal or corrosive conditions and mechanical testing right in SPL, explains Colin Judge, who, as INL’s division director for nuclear materials performance, oversees SPL and other facilities at the MFC.
SPL won’t go “hot” until January 2026, but Judge spoke with NN staff writer Susan Gallier about its capabilities as his team was moving instruments into the new facility.
Mark T. Paffett, R. Scott Willms, Charles A. Gentile, Charles H. Skinner
Fusion Science and Technology | Volume 41 | Number 3 | May 2002 | Pages 934-938
Material Interaction and Permeation | Proceedings of the Sixth International Conference on Tritium Science and Technology Tsukuba, Japan November 12-16, 2001 | doi.org/10.13182/FST02-A22722
Articles are hosted by Taylor and Francis Online.
Surface characterization studies were performed on graphite tiles used as first wall materials during DT operation of the Tokamak Fusion Test Reactor (TFTR) at the Princeton Plasma Physics Laboratory. These ex situ analysis studies revealed a number of interesting and unexpected features. In this work we examined the spatial and (where possible) the depth distribution of impurity species deposited onto the plasma facing surfaces using X-ray Photo-electron Spectroscopy (XPS) and Secondary Ion Mass Spectrometry (SIMS). This work determined that beyond the predominant species of carbon and oxygen, common impurities included silicon, boron, lithium and sulfur. Oxygen content in the plasma facing tile surfaces ranged from 20 to 50 atomic percent [excluding H-isotopes], clearly indicating an extensive zone of oxidized carbon. By contrast, carbon tile surfaces not exposed to the plasma have surface oxygen contents ranging from 2 to 6 atomic percent. Analytical measurements of the secondary impurities (B, Li, Si, S) levels were on the order of 1–4 atomic percent, (boron and lithium were injected for wall conditioning in TFTR.) The core level binding energies of these impurity species were consistent with the presence of common oxides or hydroxides (e.g., BxOy, Li2O, LiOH, Silicates). XPS measurements performed in concert with depth profiling indicated that the tile oxidized zone was significantly deeper than 1 micrometer into the (averaged) surface. Surface analytical results clearly indicate that plasma operations clearly redeposit injected impurities (Li, B) and the depth profiles and distributions of the hydrogen isotopes may be impactedand/or influenced by this deposition process.An attempt at determining hydrogen isotope concentration distributions was made using positive ion SIMS. Specific regions of some surfaces clearly indicated the presence of m/z=3 (HD, T) and m/z=15 (CH3, CHD, CT). Preliminary data examination using positive ion SIMS examination indicates that these mass markers are substantially higher in the near surface region when compared with spectra recorded deeper in the surface region. The deuterium and tritium concentrations were; however, sufficiently low or compromised bycommon isobaric interferencesthat accurate isotopic distributions using SIMS were not possible. These findings are in agreement with results reported by others. [Morimoto et al, Sun et al, reference 3 Haasz et al]
