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Colin Judge: Testing structural materials in Idaho’s newest hot cell facility
Idaho National Laboratory’s newest facility—the Sample Preparation Laboratory (SPL)—sits across the road from the Hot Fuel Examination Facility (HFEF), which started operating in 1975. SPL will host the first new hot cells at INL’s Materials and Fuels Complex (MFC) in 50 years, giving INL researchers and partners new flexibility to test the structural properties of irradiated materials fresh from the Advanced Test Reactor (ATR) or from a partner’s facility.
Materials meant to withstand extreme conditions in fission or fusion power plants must be tested under similar conditions and pushed past their breaking points so performance and limitations can be understood and improved. Once irradiated, materials samples can be cut down to size in SPL and packaged for testing in other facilities at INL or other national laboratories, commercial labs, or universities. But they can also be subjected to extreme thermal or corrosive conditions and mechanical testing right in SPL, explains Colin Judge, who, as INL’s division director for nuclear materials performance, oversees SPL and other facilities at the MFC.
SPL won’t go “hot” until January 2026, but Judge spoke with NN staff writer Susan Gallier about its capabilities as his team was moving instruments into the new facility.
Boris Yu. Goloborodsky, Vladimir V. Ovchinnikov, Vladimir A. Semionkin
Fusion Science and Technology | Volume 39 | Number 3 | May 2001 | Pages 1217-1228
Technical Paper | doi.org/10.13182/FST01-A176
Articles are hosted by Taylor and Francis Online.
The effect is studied of ion bombardment (Ar+, E = 20 keV, j = 100 A/cm2, F = 5 × 1016 to 1018 cm-2) and thermal annealing on the atomic and magnetic structure of the FePd2Au alloy after 80% cold plastic deformation and quenching from 1200°C. It is established by the Mössbauer effect and X-ray diffraction that ion irradiation at 350°C (for 1.5 to 30 min) causes formation in the disordered face-centered-cubic matrix of a long-range atomic order (of an Fe atom sublattice at an anomalously large depth up to 20 m, at an ion projected range of ~13 nm) accompanied by ferromagnetic to asperomagnetic phase transition (Tmeas = 77 K). Annealing at T = 350°C up to 30 min in the absence of irradiation does not result in any noticeable changes in the atomic and magnetic structure. Atom mobility (the ordered structure formation rate) in the course of irradiation at 350°C is approximately the same as observed in the case of annealing at 700°C.
