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Colin Judge: Testing structural materials in Idaho’s newest hot cell facility
Idaho National Laboratory’s newest facility—the Sample Preparation Laboratory (SPL)—sits across the road from the Hot Fuel Examination Facility (HFEF), which started operating in 1975. SPL will host the first new hot cells at INL’s Materials and Fuels Complex (MFC) in 50 years, giving INL researchers and partners new flexibility to test the structural properties of irradiated materials fresh from the Advanced Test Reactor (ATR) or from a partner’s facility.
Materials meant to withstand extreme conditions in fission or fusion power plants must be tested under similar conditions and pushed past their breaking points so performance and limitations can be understood and improved. Once irradiated, materials samples can be cut down to size in SPL and packaged for testing in other facilities at INL or other national laboratories, commercial labs, or universities. But they can also be subjected to extreme thermal or corrosive conditions and mechanical testing right in SPL, explains Colin Judge, who, as INL’s division director for nuclear materials performance, oversees SPL and other facilities at the MFC.
SPL won’t go “hot” until January 2026, but Judge spoke with NN staff writer Susan Gallier about its capabilities as his team was moving instruments into the new facility.
Y. Edao, H. Okitsu, H. Noguchi, S. Fukada
Fusion Science and Technology | Volume 60 | Number 3 | October 2011 | Pages 1163-1166
Blanket and Breeder Materials | Proceedings of the Ninth International Conference on Tritium Science and Technology | doi.org/10.13182/FST60-1163
Articles are hosted by Taylor and Francis Online.
We performed an experiment of H and D permeation through Li17Pb83 in the two-component (H+D) system by an unsteady permeation method to clarify interactions between H and D atoms. It was found that H and D permeate independently regardless of the H/D composition ratio in the upstream gas. Dissolution of H and D atoms into Li17Pb83 follows the Sieverts' law in the two-component system in a similar way to the single one. Diffusion of H and D in Li17Pb83 was the rate-determining step in the overall permeation process. An isotope effect of permeability between H and D was around 1.4 in the temperature range from 400°C to 700°C. The ratio of the isotope effect was in proportion to the square root of mass ratio of D to H. Tritium permeation can be estimated in a similar way.